The analysis concluded that there are only two bulk manufacturers of phosphorus, most of whose product is sold to chemical manufacturers or exported. The majority of clandestine methamphetamine laboratories seized in the U.S. utilize phosphorus chemicals as catalysts to drive the chemical conversion of ephedrine or pseudoephedrine to methamphetamine. 2013. Drug Traffic Control, Reporting and Recordkeeping Requirements. Theft/Loss ReportingImport/Export (28) Hypophosphorous acid and its salts (Including ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite and sodium hypophosphite) 6797 (29) N-phenethyl-4-piperidone (NPP) 8332 (30) Iodine: 6699 (31) Ergocristine and its salts: 8612 Recently the DEA has noted a small but increasing use of hypophosphorous acid at seized clandestine laboratories. Non-California customers must complete form QAF482. White phosphorus is much more flammable and toxic than red phosphorus. SODIUM HYPOPHOSPHITE (MONOHYDRATE) AR is not on the REACH Candidate List SODIUM HYPOPHOSPHITE (MONOHYDRATE) AR is not on the REACH Annex XIV List 15.1.2. This would be an undesired consequence, since both the white phosphorus and hypophosphorous acid methods of illicit methamphetamine production are significantly more hazardous methods. [Page 57577-57581] The authority citation for part 1310 continues to read as follows: 2. Controlled Substance Schedules DEA's research indicates that there are currently only two domestic producers of elemental phosphorus. 830 and 971. and 21 CFR parts 1310 and 1313) shall apply. DEA Forms & Applications California customers must complete form QAF481 and be advised that there is a mandatory 21-day hold prior to shipment. The United States Drug Enforcement Administration designated sodium hypophosphite as a List I chemical under 21 CFR 1310.02 effective November 17, 2001, specifically mentioning the compound together with several other salts of hypophosphorous acid. Hypophosphorous acid is commonly used by large industry as a bleaching, color stabilization or decoloring agent for plastics, synthetic fibers (primarily polyester) and chemicals. Expect a visit eventually from the DEA if you sign for any amount at all. While the manganese salt is used primarily in nylon fiber production, it also has application as a chemical intermediate. Phosphorus is also subject to Department of Transportation (DOT) hazardous material ("hazmat") regulations so that interstate and intrastate transportation require shipping papers. SODIUM HYPOPHOSPHITE … The DEA is proposing that the white and red forms of elemental phosphorus be designated as List I chemicals. SODIUM HYPOPHOSPHITE (MONOHYDRATE) AR Safety Data Sheet www.lobachemie.com 09/04/2015 2/8 2.2. The Deputy Administrator hereby certifies that this rulemaking has been drafted in a manner consistent with the principles of the Regulatory Flexibility Act (5 U.S.C. A review of chemical marketing directories identified at least 39 companies, other than the manufacturers, that claim to sell these substances. Ecological Information Environmental Fate: No information found. COVID-19 Information For reasons set out above, it is proposed that 21 CFR Part 1310 be amended as follows: 1. The DEA has not been able to identify any 'household' uses for red phosphorus, white phosphorus, or hypophosphorous acid (and its salts). Contact most popular products of manufacturers, trading companies, wholesalers & exporter directly on Made-in-China.com This notice solicits input regarding: (1) The nature of the legitimate phosphorus industry; (2) the legitimate uses of phosphorus at all levels of distribution (including industrial uses and use by individual end-users at the retail level of distribution); (3) the potential impact such regulatory controls may have on legitimate industry (particularly with respect to the impact on small businesses); (4) the potential number of individuals/firms which may be affected by increased regulatory requirements; and (5) any other information on the manner of manufacturing, distribution, consumption, storage, disposal, and uses of phosphorus by industry and others. (1) * * * The trend continues into calendar year 2000. 243663 ; Sigma-Aldrich pricing. The hypophosphites are similarly produced by very few facilities. Based on analysis of chemistry and actual illicit use, DEA finds that these three chemicals are important to the manufacture of methamphetamine and therefore meet the definition of List I chemicals. The white form is extremely flammable and toxic and must be stored and shipped in water. Both quantitative and qualitative data were invited. This rule is not a major rule as defined by Section 804 of the Small Business Regulatory Enforcement Fairness Act of 1996. 601. It also can be used as a food additive. DEA has not been able to identify any household uses for red phosphorus, white phosphorus or hypophosphorous acid and its salts. [DOCID:fr25se00-25], Control of Red Phosphorus, White Phosphorus and Hypophosphorous Acid (and Its Salts) as List I Chemicals. Interpretation Translation During 1998, the DEA identified a total of only six methamphetamine laboratories utilizing hypophosphorous acid. In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. The remaining 2% of the phosphorus (used domestically) is utilized in its elemental form (i.e. According to 1999 maritime data (as reported by the Pier Import Export Reporting Service), imports of phosphorus chemicals into the U.S. totaled 101 shipments for a total of 2,500 metric tons to 36 different firms. The Drug Enforcement Administration makes every effort to write clearly. [3][4], InChI=1S/Na.H3O2P/c;1-3-2/h;3H2,(H,1,2)/q+1;/p-1, InChI=1/Na.H3O2P/c;1-3-2/h;3H2,(H,1,2)/q+1;/p-1, Except where otherwise noted, data are given for materials in their, D. Rich & M. Smith, Electroless Deposition of Nickel, Cobalt and Iron, IBM Corp (1971), https://en.wikipedia.org/w/index.php?title=Sodium_hypophosphite&oldid=961666811, Chemical articles with multiple compound IDs, Multiple chemicals in an infobox that need indexing, Chemical articles with multiple CAS registry numbers, Articles with changed ChemSpider identifier, Pages using collapsible list with both background and text-align in titlestyle, Articles containing unverified chemical infoboxes, Creative Commons Attribution-ShareAlike License, This page was last edited on 9 June 2020, at 19:19. [Proposed Rules] Sodium hypophosphite has been indicated to react explosively when triturated with chlorates. 4.2 Most important symptoms and effects, both acute and delayed To the best of our knowledge, the chemical, physical, and toxicological properties … Based on the chemical composition of this product it is assumed that the mixture can be treated in an acclimatized biological … The primary material derived from phosphate rock is white phosphorus. crystalline) forms (white, red and black). H2O. In 1999, the DEA documented an additional 48 laboratories utilizing hypophosphorous acid. Medical Chinese dictionary (湘雅医学词典). Federal Agencies & Related Links Handlers which acquire phosphorus and convert it to non-regulated forms will not be subject to CSA regulatory requirements. Drug Disposal InformationDrug and Chemical Information Comments must be submitted on or before November 24, 2000. Reports Required by 21 CFR DEA obtained 1998 and 1999 sales data from both producers. what is sodium hypophosphite used for. The DEA has identified two manufacturers of sodium hypophosphite in the United States. Chemical Intermediate – Used as a raw material in the production of other products, including Hypophosphorous Acid. It is considered to be the sodium salt of hypophosphorous acid. 3. Find here Sodium Hypophosphite manufacturers & OEM manufacturers India. Sodium hypophosphite Names IUPAC name. Sodium Hypophosphate; sodium hyposulfate; Look at other dictionaries: Identifiers CAS Number. This rule will not result in an annual effect on the economy of $100,000,000 or more; a major increase in costs or prices; or significant adverse effects on competition, employment, investment, productivity, innovation, or on the ability of United States-based companies to compete with foreign-based companies in domestic and export markets. What Steps Has the DEA Taken To Solicit Information From the Legitimate Phosphorus Industry? Chemicals: Sodium Hypophosphite Liquid. A review of the 50 largest methamphetamine laboratories seized by DEA in 1998 was recently conducted. In case of eye contact Flush eyes with water as a precaution. Fire Extinguishing Media: Use any means suitable for extinguishing surrounding fire. It will not have a significant economic impact on a substantial number of small business entities. Chemicals: Sodium Hypophosphite Liquid Palm's SHP is blended exclusively from high purity SHP for use in electroless nickel solutions. As List I chemicals, red phosphorus, white phosphorus, and hypophosphorous acid and its salts will become subject to the chemical regulatory control provisions and civil and criminal sanctions of the CSA. Therefore, this proposed regulation will only affect the distribution of less than 2% of the industry at the end user level. National regulations Germany AwSV/VwVwS Annex reference : Water hazard class (WGK) 2, hazardous to water (Classification according to VwVwS, Annex 3; WGK No 6984) 12th Ordinance Implementing the Federal … It is a solid at room temperature, appearing as odorless white crystals. If not confined within the reaction vessel, ingestion of this poisonous gas can result in death. What Is Phosphorus Used for and How Large Is the Industry? Hypophosphorous acid is also used as a chemical intermediate in organic syntheses and as a polymerization and polycondensation catalyst. DEA's research indicates that there are currently only two domestic producers of elemental phosphorus. The Drug Enforcement Administration (DEA) has determined that these controls are necessary to prevent the diversion of these chemicals to clandestine drug laboratories. However, these materials are being distributed in small quantities via Internet online auctions and through chemical supply houses directly to consumers. 13. Many forensic laboratories do not differentiate samples as being white versus red phosphorus. Diversion Control Division  •  8701 Morrissette Drive  •  Springfield, VA 22152  •  1-800-882-9539, DEA.GOV    |     As List I chemicals, handlers of these materials will be subject to CSA chemical regulatory controls including registration, recordkeeping, reporting, and import/export requirements. Sodium hypophosphite is capable of reducing nickel ions in solution to metallic nickel on metal substrates as well as on plastic substrates. Therefore, DEA has sought information on the phosphorus chemical trade so that diversion of these chemicals may be prevented with minimal impact on legitimate industry. The analysis identified two main producers of the hypophosphites. Their information indicates that in southeastern Idaho, white phosphorus is frequently encountered in methamphetamine laboratories. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. Over 98% of the annual U.S. phosphorus demand is used in the production of these four compounds, none of which is subject to this proposed action. It is soluble in water, and easily absorbs moisture from the air. Sodium Hypophosphite (Monohydrate) CAS No 10039-56-2 MATERIAL SAFETY DATA SHEET SDS/MSDS . All transactions in those substances are subject to the reporting requirements. DEA has identified only two domestic producers of white phosphorus. While the vast majority of these laboratories utilized red phosphorus, DEA is aware that a number of seized laboratories have used white phosphorus. Sodium hypophosphite should be kept in a cool, dry place, isolated from … Sodium Hypophosphite Hydrate (DEA List I Chemical), also known as sodium phosphinate, is used for electroless nickel plating. If you have suggestions as to how to improve the clarity of this regulation, call or write Patricia M. Good, Chief, Liaison and Policy Section, Office of Diversion Control, Drug Enforcement Administration, Washington, DC 20537, telephone (202) 307-7297. Non-California customers must complete form QAF482. If red phosphorus alone is controlled, DEA has concluded that clandestine laboratory operators would rapidly move to white phosphorus and hypophosphorous acid. Sodium phosphinate. This waste material would likely be considered a chemical mixture containing phosphorus. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. As noted above, these chemicals are used as catalysts in the illicit synthesis of methamphetamine. It is a solid at room temperature, appearing as odorless white crystals. Phosphorus is covered by the Toxic Release Inventory (TRI) program, which requires an annual report to EPA listing the maximum quantity on site, the uses of the chemical, releases to the environment, and transfers offsite. Hence, this Notice proposes that these chemicals be subject to CSA regulatory controls for List I chemicals, including registration, recordkeeping, reporting, and import/export requirements as specified in 21 CFR parts 1309, 1310 and 1313. The study revealed that in those instances where the production method could be ascertained, red phosphorus was used in 87% of these laboratories. Global Sodium Hypophosphite Market was valued US$ XX Mn in 2019 and is expected to reach US$ 975.12 Mn by 2026, at a CAGR of around XX % during a forecast period.. Submit a Tip to DEA Batch: 100701/10547. It is soluble in water, alcohol, and glycerol. [[Page 57578]] What Is Phosphorus Used for and How Large Is the Industry? Publications & Manuals The DEA has identified these chemicals as being used in the illicit production of methamphetamine. With this method, a durable nickel-phosphorus film can coat objects with irregular surfaces, and can widely be used ionics, aviation and the petroleum field. Sodium Hypophosphite Monohydrate 10039-56-2 99.5-100 Not established Not established The anhydrous form of Sodium Hypophosphite has a CAS Number of 7681-53-0 [Phosphinic acid, sodium salt (1:1)] SECTION 4: FIRST AID MEASURES Inhalation: Remove affected person to fresh air; if symptoms persist seek medical attention. A few reported releasing the substance to publicly owned treatment works (i.e., wastewater treatment). An official version of this publication may be obtained directly from the Government Publishing Office (GPO). Sodium hypophosphite should be kept in a cool, dry place, isolated from oxidizing materials. Rinse mouth with water. Global Sodium Hypophosphite Market. Manufacturers, distributors, importers and exporters of white phosphorus, red phosphorus and hypophosphorous acid (and its salts) will be required to register with the DEA pursuant to 21 U.S.C. [FR Doc. (36) Red phosphorus, including white phosphorus, hypophosphorous acid and its salts, ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite, sodium hypophosphite, and phosphorous acid and its salts. English-Tamil dictionary. Other forms of phosphorus and … Source new and latest Sodium Hypophosphite products in 2020 from credible China manufacturers, suppliers and factories. DEA believes that the use of white phosphorus is under-reported. It is believed that there are few firms handling these regulated forms (i.e. CMEA (Combat Meth Epidemic Act) In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. DEA also examined Environmental Protection Agency (EPA) reporting requirements pertaining to phosphorus, hypophosphorous acid, and the hypophosphites. A limited number of other facilities manufacture phosphorus as a by-product or import phosphorus. CMEA Required Training & Self-Certification, CSOS (Controlled Substances Ordering System), Registrant Record of Controlled Substances Destroyed, Regulated Machines (Tableting and Encapsulating). Phosphorus is a nonmetallic element that can occur in three main allotropic (i.e. The primary material derived from phosphate rock is white phosphorus. Hypophosphorous acid and sodium hypophosphite are List I and have no "threshold" quantity. Federal Register Notices, National Prescription Drug Take Back Day H2O. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. Companies creating MSDSs for chemicals are likely to manufacture or distribute the chemicals. E-commerce Initiatives It is also used as a reducing agent, analytical reagent, polymerization catalyst, polymer stabilizer, and fire retardant. Sodium Hypophosphite (Monohydrate) CAS No 10039-56-2 MATERIAL SAFETY DATA SHEET SDS/MSDS . It is a critical ingredient of electroless nickel plating solutions. JUSTICE.GOV    |     as red phosphorus or white phosphorus) or used to produce all other phosphorus chemicals including sodium hypophosphite and hypophosphorous acid. Sodium hypophosphite should be kept in a cool, dry place, isolated from oxidizing materials. Medical Missions As Part of This Proposed Rulemaking, the DEA Again Invites Input Regarding the Legitimate Uses for These Chemicals. The sodium salt is used primarily in electroless nickel plating. In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. Sodium hypophosphite monohydrate can be used as a: • Reducing agent in the synthesis of nickel nanoparticles (NiNP) from nickel acetate tetrahydrate under microwave irradiation. Because of their use and importance in the illicit manufacture of methamphetamine, a Schedule II controlled substance, the DEA is proposing the addition of red phosphorus, white phosphorus (also known as yellow phosphorus) and hypophosphorous acid (and its salts) as List I chemicals. This notice proposes, therefore, that no threshold be established for domestic and international transactions. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. BILLING CODE 4410-09-P. NOTICE: This is an unofficial version. Therefore, no actions were deemed necessary under the provisions of the Unfunded Mandates Reform Act of 1995. Sodium hypophosphite is a colorless hygroscopic solid, soluble in water. Resources 5 min read . It is used as a water treatment agent and as a meat preservative. The United StatesDrug Enforcement Administration (DEA) maintains lists regarding the classification of illicit drugs (see DEA Schedules). (DEA List I Chemical) 30410 | 10039-56-2. 601 et seq.). Salts of hypophosphorous acid are known as hypophosphite salts. Sodium Hypophosphite Monohydrate 10039-56-2 231-669-9 7640mg / kg Oral - rat Not established SECTION 12: ECOLOGICAL INFORMATION 12.1 No data are available on the adverse effects of this material on the environment. It is a solid at room temperature, appearing as odorless white crystals. Electroless Nickel (EN) – Sodium Hypophosphite (SHP) acts as a reducing agent to supply the electrons necessary for the EN process.The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. White phosphorus is primarily used to produce phosphoric acid and other phosphorus compounds including phosphorus trichloride and phosphorous pentasulfide and phosphorus pentoxide. It is considered to be the sodium salt of hypophosphorous acid. The MSDSs located for the hypophosphites indicate. In 1998, 53 facilities reported to EPA for phosphorus. This rule will not result in the expenditure by state, local, and tribal governments, in the aggregate, or by the private sector, of $100,000,000 or more in any one year, and will not significantly or uniquely affect small governments. What Regulatory Controls Will Apply to These Chemicals? H 2 O. Sodium Hypophosphite (7681-53-0) No No None 12. California customers must complete form QAF481 and be advised that there is It is common to find 500 ml bottles of hypophosphorous acid or multi-ounce quantities of red phosphorus repackaged in unlabeled bags at seized laboratories. Industrial uses of red phosphorus include the manufacture of pyrotechnics, safety matches, phosphoric acid and other phosphorus compounds, fertilizers, incendiary shells, smoke bombs, tracer bullets, and pesticides. phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) EC Number: 600-090-7 CAS Number: 10039-56-2 Molecular formula: NaH4PO3 IUPAC Name: phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) Om inget annat anges ges data för material i deras standardtillstånd (vid 25 ° C, 77 kF). Other forms of phosphorus and other phosphorus chemicals are manufactured from white phosphorus. From 1997 through the first quarter of 2000, 86 methamphetamine laboratories were seized in this region of Idaho. (25) Red phosphorus--6795 H 2 O. It is soluble in water, and easily absorbs moisture from the air. Sodium hypophosphite is mainly used for electroless nickel-plating. red phosphorus, white phosphorus and hypophosphorous acid and its salts.) This data indicated that most all the material appeared to be for large industrial uses. The CSA, therefore, provides the Attorney General with authority to establish a threshold amount for "listed chemicals" if the Attorney General so elects. 822 and 823 and 21 CFR part 1309. View detailed Import data, price, monthly trends, major importing countries, major ports of sodium hypophosphite under HS Code 2835 Palm's SHP is blended exclusively from high purity SHP for use in electroless nickel solutions. The two most common salts of hypophosphorous acid are sodium hypophosphite and manganese hypophosphite. Additionally, hypophosphorous acid is covered in interstate commerce. SDS; Sodium hypophosphite monohydrate. It is a solid at room temperature, appearing as odorless white crystals. FOR FURTHER INFORMATION CONTACT: Frank L. Sapienza, Chief, Drug and Chemical Evaluation Section, Office of Diversion Control, Drug Enforcement Administration, Washington D.C. 20537 at (202) 307-7183. Mailing Addresses (ii) Red phosphorus The Department of Justice does not endorse the organizations or views represented by this site and takes no responsibility for, and exercises no control over, the accuracy, accessibility, copyright or trademark compliance or legality of the material contained on this site. REGULATIONS.GOV, DOJ Legal Policies and Disclaimers    |    DOJ Privacy Policy    |    FOIA    |    Section 508 Accessibility. Sodium hypophosphite is the most commercially available salt and is distributed in a white crystalline form. In case of eye contact Flush eyes with water as a precaution. While chemical mixtures are currently exempt from CSA chemical regulatory requirements, the DEA is preparing regulations pertaining to such mixtures. 1272/2008 [CLP] Extra labelling to displayExtra classification(s) to display H 2 O. It is a common reducing agent for metal plating. It is soluble in water, and easily absorbs moisture from the air. H 2 O. Therefore, the manufacture of methamphetamine requires only small quantities of these chemicals. This regulation meets the applicable standards set forth in Sections 3(a) and 3(b)(2) of Executive Order 12988, Civil Justice Reform. This action has been analyzed in accordance with the principles and criteria in Executive Order 13132, and it has been determined that this rule does not have sufficient federalism implications to warrant the preparation of a Federalism Assessment. 2 NaPO 2 H 2 → PH 3 + Na 2 HPO 4. Twenty-one of the 53 facilities reporting phosphorus under TRI sent phosphorus offsite to 30 separate places for treatment as waste. Sodium Hypophosphite 次磷酸钠. Significant Guidance Documents How Many Importers and Exporters Are Potentially Affected? Except where otherwise noted, data are given for materials in their standard state (at 25 °C [77 °F], 100 kPa). Sodium Hypophosphite is used in formulating many pharmaceutical products. El-Ahraf A, Van Willis W, Vinjamoori DV. Hypophosphorous acid shipments should be documented, but shipments of the hypophosphites may not be. SUMMARY: The Comprehensive Drug Abuse Prevention and Control Act (hereinafter the "Controlled Substances Act" or "CSA") provides the Attorney General with the authority to specify by regulation, additional chemicals as "List I" chemicals if they are used in the manufacture of a controlled substance in violation of the CSA and are important to the manufacture of the controlled substance. 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